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December 02-03, 2019 | Dubai, UAE

Oil & Gas

2

nd

International Conference and Expo on

Journal of Industrial and Environmental Chemistry | Volume 3

The influence of the quality of deep samples on the results of studies of the phase

behavior of paraffins and formation oil asphaltenes

Stanislav Fedorovskiy

GAZPROM NEFT Science & Technology Centre, Russia

T

he paper illustrates the influence of the quality of

downhole samples on the results of studies of the phase

behavior of paraffins and asphaltenes in reservoir oil. The

results of studies of a conditionally representative sample of

reservoir oil and deep samples taken under multiphase flow

conditions (with different volumes of free gas, formation

water and solid phase of asphaltenes, resins and paraffins in

the sampler) were compared. For each sample, a set of PVT

studies was carried out according to all required standards

– PVT test, flash separation, determination of viscosity and

density. Phase behavior of paraffins and asphaltenes was

studied by methods of acoustic resonance (registration of

the moment of phase transition), high pressure microscopy

(determination of the number and geometric dimensions

of solid phase particles), gravimetric and filtration methods

(determination of the group composition of the solid phase).

To prepare samples of oil with free gas in the chambers,

a procedure was carried out to release free gas to the

current bubble-point pressure. The results of the analysis

revealed that the procedure of free gas release has little

effect on the PVT-characteristics of reservoir fluid samples.

However, it is not possible to study the phase behavior of

paraffins and asphaltenes, since the deviation of different

parameters reaches 70% (the content of asphaltenes, resins

and paraffins; paraffin saturation temperature; asphaltene

saturation pressure, etc.) As a result, the sample of fluids with

multiphase flow conditions, if it is impossible to use other

methods, may be acceptable for a standard PVT-analysis. But

it is not possible to study the phase behavior of paraffins and

asphaltenes for such samples, since these studies are highly

dependent on the quality of sampling.

Speaker Biography

Stanislav Fedorovskiy is the team leader of reservoir fluids studies of the

GAZPROM NEFT Science and Technology Center. By academic professional

education, he is a refinery engineer, but his career is all about studying

reservoir fluids. He worked as an engineer in a PVT-laboratory of one

of the research centers of PJSC Gazprom, where he mastered all the

fundamental knowledge and skills in the culture of working with downhole

and separator samples. Next, he became the head of the laboratory of

physical and chemical analysis of degassed (wellhead) samples in the

research center of JSC SibNIINP, having gained experience of research and

management of the team, he went to work directly at the GAZPROMNEFT

Science and Technology Center, where for 4 years he has made the way

from leading specialist to team leader. The specificity of their work lies in

the absolute diversity of properties and phase states of the fluid – from

heavy oil to supercritical fluids.

e:

fedorovskiy.sa@gazpromneft-ntc.ru

Stanislav Fedorovskiy

, J Ind Environ Chem, Volume:3

DOI: 10.35841/2591-7331-C3-014