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Page 32
allied
academies
November 22-23, 2018 | Paris, France
Journal of Materials Science and Nanotechnology | Volume: 2
Materials Physics and Materials Science
International Conference on
Effect of sintering on formation and structure of nanocrystalline La
0.1
C
0.9
MnO
3
perovskite
Mohamed Hegazy
Zagazig University, Egypt
N
anocrystalline La
0.1
C
0.9
MnO
3
perovskite been synthesized
employing co-precipitation technique. X-Ray Diffraction
(XRD) and Fourier-transform Infrared spectroscopy (FTIR)
analysis were used to explore the structural features and
calculate lattice parameter values for all the compositions
(as prepared, sintered at 200, 400, 600, 800 and 1000 0C for
3h). Formation of nanoparticles was revealed by transmission
electronmicroscopy (TEM). The elemental analysis as obtained
by EDAX is in close agreement with the expected composition
from the stoichiometry of reactant solutions used. Increasing
sintering temperature enhances theperovskite structure to800
0C. Theperovskite structure is distortedabove this temperature.
Crystallite size was determined by three method Scherrer,
Williamson Hall, and Warren Averbach to be in ranging from
33 to 86nm.
e:
mghozza2@yahoo.com